Ethylamine → HCID 178503882, compound

HRID 1711172Notes

Reaction equation

[CH2:1]([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])[CH3:2].[CH:10]1(N)CC1.C(N)C>>[CH:1]1([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])[CH2:10][CH2:2]1

Participants

Reactant 3

HCID 6341Ethylamine

HCID 69828Cyclopropylamine

HCID 178464595HCID 178464595, compound

Product 1

HCID 178503882HCID 178503882, compound

Procedure

1-Cyclopropyl-2-methyl-3-cyanoisothiourea was prepared following the same procedure as for 1-ethyl-2-methyl-3-cyanoisothiourea (see EXAMPLE 250) except cyclopropylamine was used in lieu of ethylamine. 1H NMR (CDCl3) δ 0.66-0.76 (m, 2H), 0.83-0.92 (m, 2H), 2.43 (s, 3H), 2.64 (br s, 1H), 6.78 (br s, 1H).

Sources & evidence

ORD record: ord-6a1ca9b6fac245778f94f363ac3bbc74
Source dataset: uspto-grants-2010_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07790747B2

Reaction notes

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