Ethylamine → HCID 178503906, compound

HRID 1711173Notes

Reaction equation

[CH2:1]([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])[CH3:2].[CH:10](N)(C)C.C(N)C>>[CH:1]([NH:3][C:4](=[N:7][C:8]#[N:9])[S:5][CH3:6])([CH3:10])[CH3:2]

Participants

Reactant 3

HCID 6341Ethylamine

HCID 6363Isopropylamine

HCID 178464595HCID 178464595, compound

Product 1

HCID 178503906HCID 178503906, compound

Procedure

1-Isopropyl-2-methyl-3-cyanoisothiourea was prepared following the same procedure as for 1-ethyl-2-methyl-3-cyanoisothiourea (see EXAMPLE 250) except isopropylamine was used in lieu of ethylamine. 1H NMR (CDCl3) δ 1.25 (d, 6H, J=6 Hz), 2.49 (br s, 3H), 3.84 (br s, 1H), 6.22 (br s, 1H).

Sources & evidence

ORD record: ord-1dd2aaf09e35493ba9187dc906c54955
Source dataset: uspto-grants-2010_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07790747B2

Reaction notes

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