HRID1711243

反应详情

EQUATION

反应方程式

HRID 1711243 的结构方程式

PROCEDURE

实验过程

The title compound was prepared by the Suzuki coupling procedure of Example 11, step (e) using 4-amino-3-bromo-benzamide (as prepared in the previous step, 500 mg, 2.32 mmol), and cyclohexane-1-enyl boronic acid (322 mg, 2.56 mmol). The mixture was purified by trituration with DCM to afford the title compound (382 mg, 76%) as a yellow solid. Mass spectrum (ESI, m/z): Calcd. for C13H16N2O, 217.1 (M+H), found 217.2.

WORKUP

后处理

  1. customThe title compound was prepared by the Suzuki coupling procedure of Example 11, step (e)
  2. customThe mixture was purified by trituration with DCM