4-Aminophenethyl alcohol → HCID 58754883, compound

HRID 1711263Notes

Reaction equation

HRID 1711263 reaction equation
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][OH:10])=[CH:4][CH:3]=1.[C:11]1(B(O)O)[CH2:16][CH2:15][CH2:14][CH2:13][CH:12]=1>>[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][OH:10])=[CH:4][C:3]=1[C:11]1[CH2:16][CH2:15][CH2:14][CH2:13][CH:12]=1

Participants

3

Reactant 2

HCID 669044-Aminophenethyl alcoholHCID 38629021-Cyclohexenylboronic acid

Product 1

HCID 58754883HCID 58754883, compound

Procedure

The title compound was prepared by Suzuki coupling of 2-(4-amino-phenyl)-ethanol (prepared in the previous step) and 1-cyclohexen-1-yl-boronic acid according to the procedure of Example 44, step (b). Mass spectrum (ESI, m/z): Calcd. for C14H19NO, 218.1 (M+H), found 218.1.

Sources & evidence

ORD record
ord-a1fc297edf7b469d81b9787fb2b22fac
Source dataset
uspto-grants-2010_09
Patent number
US07790724B2

Reaction notes

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