HRID1711297

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2734895

5-Bromo-2-methoxypyridine

C6H6BrNO

结构：CC1(C)OB(c2ccc([N+](=O)[O-])cc2)OC1(C)C

HCID2773555

4,4,5,5-tetramethyl-2-(4-nitrophenyl)-1,3,2-dioxaborolane

C12H16BNO4

PRODUCTS

生成物

HCID58754845

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

结构：c1ccc([P](c2ccccc2)(c2ccccc2)[Pd]([P](c2ccccc2)(c2ccccc2)c2ccccc2)([P](c2ccccc2)(c2ccccc2)c2ccccc2)[P](c2ccccc2)(c2ccccc2)c2ccccc2)cc1

催化剂HCID178418397

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4,4,5,5-tetramethyl-2-(4-nitro-phenyl)-[1,3,2]dioxaborolane (899 mg, 3.60 mmol), 5-bromo-2-methoxy-pyridine (616 mg, 3.28 mmol) and Pd(PPh3)4 (380 mg, 0.360 mmol) according to the procedure in Example 44, step (b) (615 mg, 94%). Mass spectrum (ESI, m/z): Calcd. for C12H10N2O3, 231.0 (M+H), found 231.2.