HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 58754803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | HCID 68509947 | HCID 68509947 | — |
| Product | HCID 58754803 | HCID 58754803 | — |
Reaction Steps
The title compound was prepared from 4-amino-3-(4,4-dimethyl-cyclohex-1-enyl)-benzonitrile (as prepared in the previous step, 245 mg, 1.08 mmol), and azidotrimethylstannane (246 mg, 1.19 mmol) according to the procedure in Example 52, step (c) (363 mg, 78%). Mass spectrum (ESI, m/z): Calcd. for C15H19N5, 270.1 (M-SnMe3+2H), found 270.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790724B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-13dcc7260e7a4cbcba0e92c6103969f0 |
| Source note | uspto-grants-2010_09 |