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HRID1711747

反应详情

EQUATION

反应方程式

HRID 1711747 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)Cl
HCID31297

Methanesulfonyl chloride

CH3ClO2S

结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)N1CCC(O)C1
HCID58673070

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)Oc1ccc(S(C)(=O)=O)cc1C(=O)N1CCC(OS(C)(=O)=O)C1
HCID58673069

未命名化合物

收率 99%

PROCEDURE

实验过程

Prepared in analogy to Example 3(b) from rac-(3-hydroxy-pyrrolidin-1-yl)-(2-isopropoxy-5-methanesulfonyl-phenyl)-methanone (Example 9(a)) and methanesulfonyl chloride. The crude material was purified by partitioning between dichoromethane and water to yield the title compound as a yellow oil (yield 99%). MS (m/e): 406.4 (M+H+, 100%).

WORKUP

后处理

  1. customThe crude material was purified
  2. customby partitioning between dichoromethane and water