HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl bromide → 4-Allyloxy-3-nitrobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | 4-Hydroxy-3-nitrobenzaldehyde | HCID 18169 | — |
| Product | 4-Allyloxy-3-nitrobenzaldehyde | HCID 22401152 | — |
Reaction Steps
Analogously to Method F, 25 g of 4-hydroxy-3-nitrobenzaldehyde and 25.1 ml of allyl bromide are reacted. The title compound is obtained as a slightly yellowish solid. Rf=0.30 (1:2 EtOAc-heptane). Rt=4.00.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07790715B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-1c9822a86c62464eb41a7a1ef5f32e09 |
| Source note | uspto-grants-2010_09 |