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HRID1712382

反应详情

EQUATION

反应方程式

HRID 1712382 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCC(c2ccc(O)cc2)C(O)C1
HCID21713087

未命名化合物

结构：COc1ccccc1CCOCCOS(=O)(=O)c1ccc(C)cc1
HCID86609999

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccccc1CCOCCOc1ccc(C2CCN(C(=O)OC(C)(C)C)CC2O)cc1
HCID68506643

未命名化合物

PROCEDURE

实验过程

Analogously to Method I, 2.80 g of tert-butyl 3-hydroxy-4-(4-hydroxyphenyl)piperidine-1-carboxylate and 3.71 g of 2-[2-(2-methoxyphenyl)ethoxy]ethyl toluene-4-sulphonate (Example 45b) are reacted. The title compound is obtained as a colourless oil. Rf=0.47 (1:1 EtOAc-heptane); Rt=5.11.