HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzaldehyde → HCID 59463696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzaldehyde | HCID 541 | — |
| Reactant | Furfural | HCID 7362 | — |
| Reactant | Ethyl cyanoacetate | HCID 7764 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Product | HCID 59463696 | HCID 59463696 | 39.3% |
Reaction Steps
In analogy to GP 1, reaction of 1.85 g ammonium acetate (24 mmol, 8 eq.), 0.28 ml ethyl cyanoacetate (3 mmol, 1 eq.), 330 mg furan-2-carbaldehyde (3 mmol, 1 eq.), and 453 mg 4-nitrobenzaldehyde (3 mmol, 1 eq.) yielded 362 mg product (39% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795264B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-947212d05d86469dbc6306b625633331 |
| Source note | uspto-grants-2010_09 |