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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1713010Generated: October 31, 2026

4-Nitrobenzaldehyde → HCID 59463696, compound

https://huagongshe.com/reaction/1713010

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-NitrobenzaldehydeHCID 541—
ReactantFurfuralHCID 7362—
ReactantEthyl cyanoacetateHCID 7764—
ReactantAmmonium AcetateHCID 517165—
ProductHCID 59463696HCID 5946369639.3%

Reaction Steps

In analogy to GP 1, reaction of 1.85 g ammonium acetate (24 mmol, 8 eq.), 0.28 ml ethyl cyanoacetate (3 mmol, 1 eq.), 330 mg furan-2-carbaldehyde (3 mmol, 1 eq.), and 453 mg 4-nitrobenzaldehyde (3 mmol, 1 eq.) yielded 362 mg product (39% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07795264B2
Source datasetuspto-grants-2010_09
ORD IDord-947212d05d86469dbc6306b625633331
Source noteuspto-grants-2010_09