1-Bromopentane → HCID 67457474, compound

HRID 1713268Notes

Reaction equation

HRID 1713268 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][C:11]([CH2:14][NH:15][C:16](=[O:22])[O:17][C:18]([CH3:21])([CH3:20])[CH3:19])=[CH:10][CH:9]=1.Br[CH2:24][CH2:25][CH2:26][CH2:27][CH3:28]>>[CH2:24]([O:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[CH:13]=[CH:12][C:11]([CH2:14][NH:15][C:16](=[O:22])[O:17][C:18]([CH3:19])([CH3:21])[CH3:20])=[CH:10][CH:9]=1)[CH2:25][CH2:26][CH2:27][CH3:28]

Participants

3

Reactant 2

HCID 80571-BromopentaneHCID 67457935HCID 67457935, compound

Product 1

HCID 67457474HCID 67457474, compound

Procedure

The title compound was prepared in a similar manner to that described in Reference Example 20 using tert-butyl N-(2′-hydroxybiphenyl-4-ylmethyl)carbamate instead of tert-butyl N-(3′-hydroxybiphenyl-4-ylmethyl)carbamate and 1-bromopentane instead of 1-bromopropane.

Sources & evidence

ORD record
ord-e2cb23339fa148d08756fe9d051a2154
Source dataset
uspto-grants-2010_09
Patent number
US07795236B2

Reaction notes

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