HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(tert-Butoxycarbonylaminomethyl)phenylboronic acid, pinacol ester → Tert-butyl n-(3'-benzyloxy-5'-dimethylcarbamoylbiphenyl-4-ylmethyl)carbamate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(tert-Butoxycarbonylaminomethyl)phenylboronic acid, pinacol ester | HCID 3415442 | — |
| Reactant | 3-Benzyloxy-5-hydroxy-N,N-dimethylbenzamide | HCID 67456467 | — |
| Product | Tert-butyl n-(3'-benzyloxy-5'-dimethylcarbamoylbiphenyl-4-ylmethyl)carbamate | HCID 67454928 | — |
Reaction Steps
The title compound was prepared in a similar manner to that described in Reference Example 58 using 3-benzyloxy-5-hydroxy-N,N-dimethylbenzamide instead of 4-hydroxy-3-methoxybenzaldehyde and tert-butyl N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolane-2-yl)bezyl]carbamate instead of phenylboronic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795236B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-57ace74f7efb4a0ab833679c0cc42273 |
| Source note | uspto-grants-2010_09 |