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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1713380Generated: November 1, 2026

Trifluoroacetic acid → HCID 59463765, compound

https://huagongshe.com/reaction/1713380

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 59463762HCID 59463762—
SolventDichloromethaneHCID 6344—
ProductHCID 59463765HCID 5946376565%

Reaction Steps

TFA (2 ml) was added to a solution of compound 42 (100 mg, 0.18 mmol) in dichloromethane (4 ml) and the solution was stirred at room temperature. After 30 min the solvents were evaporated in vacuo and the afforded residue was purified by column chromatography on silica gel which gave the title compound (52 mg, 65%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07795270B2
Source datasetuspto-grants-2010_09
ORD IDord-42437e22a4a9426ca8b5b017153d67ff
Source noteuspto-grants-2010_09