HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 23121936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | HCID 86761172 | HCID 86761172 | — |
| Product | HCID 23121936 | HCID 23121936 | 84% |
Reaction Steps
To 1,1-dimethylethyl [[3-[[[(tetrahydro-3-oxo-1,1-diphenyl-3H-oxazolo[3,4-a]pyrazin-7(1H)-yl)carbonyl]amino]methyl]phenyl]methyl]carbamate (0.12 g, 0.22 mmol) was added trifluoroacetic acid (1.5 mL), and the mixture was stirred at room temperature for 2 hours. To the reaction solution was added diisopropyl ether, the precipitated powder was collected by filtration and dried to obtain the title compound (0.11 g, yield 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07795267B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-a9d6ec3eb4b3416db99daf343fbfb8f6 |
| Source note | uspto-grants-2010_09 |