4-(3-(Dimethylamino)propoxy)aniline → HCID 58923526, compound

HRID 1713690Notes

Reaction equation

HRID 1713690 reaction equation
[N:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][CH2:10]N2CCCC2)=[CH:6][CH:5]=1)=[C:2]=[S:3].[CH3:18][N:19]([CH3:31])[CH2:20]CCOC1C=CC(N)=CC=1>>[N:1]([C:4]1[CH:5]=[CH:6][C:7]([O:8][CH2:9][CH2:10][CH2:18][N:19]([CH3:31])[CH3:20])=[CH:16][CH:17]=1)=[C:2]=[S:3]

Participants

3

Reactant 2

HCID 100584694-(3-(Dimethylamino)propoxy)anilineHCID 118461221-(2-(4-Isothiocyanatophenoxy)ethyl)pyrrolidine

Product 1

HCID 58923526HCID 58923526, compound

Procedure

The title compound is prepared as described in Example 1 for 1-[2-(4 isothiocyanato-phenoxy)-ethyl]-pyrrolidine but using 4-(3-dimethylamino-propoxy)-phenylamine. Title compound: ES-MS: 237.1 [M+H]+; single peak at tR=6.91 min (System 1).

Workup

  1. customThe title compound is prepared

Sources & evidence

ORD record
ord-917976de46da4f738d7778d8a2ed5fe4
Source dataset
uspto-grants-2010_09
Patent number
US07795288B2

Reaction notes

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