4-(2-(Diethylamino)ethoxy)aniline → 4-(2-Diethylaminoethoxy)phenylisothiocyanate

HRID 1713692Notes

Reaction equation

HRID 1713692 reaction equation
[N:1]([C:4]1[CH:17]=[CH:16][C:7]([O:8][CH2:9][CH2:10][N:11]2[CH2:15][CH2:14][CH2:13][CH2:12]2)=[CH:6][CH:5]=1)=[C:2]=[S:3].C(N(CC)CCOC1C=CC(N)=CC=1)C>>[CH2:15]([N:11]([CH2:12][CH3:13])[CH2:10][CH2:9][O:8][C:7]1[CH:6]=[CH:5][C:4]([N:1]=[C:2]=[S:3])=[CH:17][CH:16]=1)[CH3:14]

Participants

3

Reactant 2

HCID 4189324-(2-(Diethylamino)ethoxy)anilineHCID 118461221-(2-(4-Isothiocyanatophenoxy)ethyl)pyrrolidine

Product 1

HCID 226409854-(2-Diethylaminoethoxy)phenylisothiocyanate

Procedure

The title compound is prepared as described in Example 1 for 1-[2-(4-isothiocyanato-phenoxy)-ethyl]-pyrrolidine but using 4-(2-diethylamino-ethoxy)-phenylamine. Title compound: ES-MS: 251.1 [M+H]+; single peak at tR=6.99 min (System 1).

Workup

  1. customThe title compound is prepared

Sources & evidence

ORD record
ord-e55002b250844cde9ef44271d3b232e1
Source dataset
uspto-grants-2010_09
Patent number
US07795288B2

Reaction notes

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