Aluminium lithium hydride → cis-Benzyl-(3,8-dimethyl-2,3,4,4a,9,9a-hexahydro-1H-3-aza-fluoren-6-yl)-amine

Participants

Reaction Steps

The title compound (5.0 mg, 0.016 mmol) was prepared by following the procedure of step B of example 17 from crude cis-6-benzylamino-8-methyl-1,2,4,4a,9,9a-hexahydro-3-aza-fluorene-3-carboxylic acid ethyl ester (66 mg, 0.18 mmol) and LiAlH4 (27 mg, 0.73 mmol) in THF (1 mL): MS (ES) 307.2 (M+H).

Provenance & Evidence