Dimethylamine → HCID 59235880, compound

HRID 1714696Notes

Reaction equation

HRID 1714696 reaction equation
[CH3:1][NH:2][CH3:3].[CH2:4]=O.[Cl:6][C:7]1[CH:8]=[C:9]([CH:12]=[CH:13][C:14]=1[OH:15])[CH:10]=[O:11]>C(O)C>[Cl:6][C:7]1[CH:8]=[C:9]([CH:12]=[C:13]([CH2:1][N:2]([CH3:4])[CH3:3])[C:14]=1[OH:15])[CH:10]=[O:11]

Participants

5

Reactant 3

HCID 674DimethylamineHCID 712FormaldehydeHCID 170223-Chloro-4-hydroxybenzaldehyde

Product 1

HCID 59235880HCID 59235880, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

11.5 g (0.96 mol) of a 40% aqueous dimethylamine solution were added to 7.7 g (0.96 mol) of a 37% aqueous formaldehyde solution in 60 ml of ethanol. Then 10.0 g (0.64 mol) of 3-chloro-4-hydroxybenzaldehyde were added thereto. The reaction mixture was refluxed for 30 minutes and then stirred for 24 hours at room temperature. The precipitated white solid was filtered out and dried.

Workup

  1. temperatureThe reaction mixture was refluxed for 30 minutes
  2. filtrationThe precipitated white solid was filtered out
  3. customdried

Sources & evidence

ORD record
ord-7a08b8d732db484daea6b40eb500a0b7
Source dataset
uspto-grants-2010_09
Patent number
US07799096B2

Reaction notes

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