HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-(benzyloxy)-2,3,4,5-tetrahydro-1H-3-benzazepine → 7-[(2-Fluoro-4-iodophenyl)oxy]-2,3,4,5-tetrahydro-1H-3-benzazepine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-(benzyloxy)-2,3,4,5-tetrahydro-1H-3-benzazepine | HCID 57437617 | — |
| Reactant | 1,1-Dimethylethyl 7-[(2-fluoro-4-Iodophenyl)oxy]-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate | HCID 58984572 | — |
| Product | 7-[(2-Fluoro-4-iodophenyl)oxy]-2,3,4,5-tetrahydro-1H-3-benzazepine | HCID 58984576 | — |
Reaction Steps
The title compound was prepared from 1,1-dimethylethyl 7-[(2-fluoro-4-iodophenyl)oxy]-1,2,4,5-tetrahydro-3H-3-benzazepine-3-carboxylate (E274, Step 3) using an analogous method to that described for Description 2 (D2). MS (ES+) m/e 384 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07799773B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-721dc09b45764a3bb7c488c2c65cc7eb |
| Source note | uspto-grants-2010_09 |