Potassium cyanate → HCID 59028793, compound

HRID 1715067Notes

Reaction equation

HRID 1715067 reaction equation
[C:1]1([S:7]([C:10]2[CH:11]=[C:12]3[C:17](=[CH:18][CH:19]=2)[C:16]([CH2:20][NH2:21])=[CH:15][CH:14]=[CH:13]3)(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[O-:22][C:23]#[N:24].[K+]>O>[C:1]1([S:7]([C:10]2[CH:11]=[C:12]3[C:17](=[CH:18][CH:19]=2)[C:16]([CH2:20][NH:21][C:23]([NH2:24])=[O:22])=[CH:15][CH:14]=[CH:13]3)(=[O:9])=[O:8])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

Participants

4

Reactant 2

HCID 11378442Potassium cyanateHCID 59028770C-(6-Benzenesulfonyl-naphthalen-1-yl)-methylamine

Product 1

HCID 59028793HCID 59028793, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
60 °C

Procedure

C-(6-Benzenesulfonyl-naphthalen-1-yl)-methylamine and potassium cyanate are added to stirring water, and the mixture is heated to 60° C., then cooled to room temperature. The resulting precipitate is collected by filtration, washed with cold water, and dried under vacuum to give (6-benzenesulfonyl-naphthalen-1-ylmethyl)-urea.

Workup

  1. temperaturecooled to room temperature
  2. filtrationThe resulting precipitate is collected by filtration
  3. washwashed with cold water
  4. customdried under vacuum

Sources & evidence

ORD record
ord-346062c69e324111a9a5d8e10f51615f
Source dataset
uspto-grants-2010_09
Patent number
US07799797B2

Reaction notes

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