HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → HCID 59323901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | HCID 59323907 | HCID 59323907 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59323901 | HCID 59323901 | — |
Reaction Steps
Dry DCM (10 ml) is added to 1-[4-(2-amino-4-methyl-thiazol-5-yl)-2-fluoro-phenyl]-ethanone (0.25 g, 1.0 mmol) and CDI (0.259 g, 1.6 mmol) and the mixture is heated at reflux for 4 hours. The resulting suspension is filtered and dried under vacuum to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07799810B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-a94a4c45cdae427f930bcdf23140a05e |
| Source note | uspto-grants-2010_09 |