1,2-Bis(4-methylphenyl)-1,2-ethanedione → HCID 5052632, compound

Participants

Reaction Steps

1.84 g (12 mmol) of 2,3-diaminonitrobenzene and 2.38 g (10 mmol) of 4,4′-dimethylbenzil were dissolved in 40 g of a mixed solvent of acetic acid and methanol (1:1) and reacted at a reaction temperature of 80° C. for 4 hours. After completion of the reaction, the solvent was removed and the resulting reaction product was extracted by means of a silica gel column.

Provenance & Evidence