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HRID1716229

反应详情

EQUATION

反应方程式

HRID 1716229 的结构方程式

REACTANTS

反应物

2
结构：O=C(CCl)N1CCCc2ccccc21
HCID240137

2-Chloro-1-(3,4-dihydroquinolin-1(2H)-yl)ethan-1-one

C11H12ClNO

结构：Sc1nc(-c2ccccc2)c(-c2ccccc2)[nH]1
HCID178527825

未命名化合物

PRODUCTS

生成物

1
结构：O=C(CSc1nc(-c2ccccc2)c(-c2ccccc2)[nH]1)N1CCCc2ccccc21
HCID23887493

未命名化合物

收率 26%

PROCEDURE

实验过程

The title compound was synthesized according to General Procedure A using compound 4 as the electrophile and 4,5-diphenyl-1H-imidazole-2-thiol as the nucleophile to yield 19 as a off-white solid (26%): MS m/z: 426 (M+H)+. Anal. Calcd. For, C26H23N3OS.0.2H2O: C, 72.77; H, 5.50; N, 9.79; S, 7.47. Found: C, 72.58; H, 5.33; N, 9.74; S, 7.48.

WORKUP

后处理

  1. customThe title compound was synthesized