3-Nitrobenzenesulfonyl chloride → HCID 68708472, compound

HRID 1716357Notes

Reaction equation

HRID 1716357 reaction equation
[CH3:1][O:2][C:3]1[C:4]([CH3:12])=[CH:5][N:6]2[C:11]=1[CH:10]=[CH:9][CH:8]=[CH:7]2.[N+:13]([C:16]1[CH:17]=[C:18]([S:22](Cl)(=[O:24])=[O:23])[CH:19]=[CH:20][CH:21]=1)([O-:15])=[O:14]>>[CH3:1][O:2][C:3]1[C:4]([CH3:12])=[C:5]([S:22]([C:18]2[CH:19]=[CH:20][CH:21]=[C:16]([N+:13]([O-:15])=[O:14])[CH:17]=2)(=[O:23])=[O:24])[N:6]2[C:11]=1[CH:10]=[CH:9][CH:8]=[CH:7]2

Participants

3

Reactant 2

HCID 84763-Nitrobenzenesulfonyl chlorideHCID 113211231-methoxy-2-methylindolizine

Product 1

HCID 68708472HCID 68708472, compoundYield 98%

Procedure

This compound is prepared according to the protocol described for the example above, by sulphonylation of 1 g (6.2 mmol) of 1-methoxy-2-methylindolizine with 3-nitrobenzenesulphonyl chloride. 540 mg of a yellow oil are obtained.

Workup

  1. customThis compound is prepared

Sources & evidence

ORD record
ord-fefbdfaa82784c8497f44c17cbfcf548
Source dataset
uspto-grants-2010_09
Patent number
US07803811B2

Reaction notes

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