Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | O-Methyltyramine | HCID 4657 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68426881 | HCID 68426881 | — |
Reaction Steps
4-Methoxyphenethylamine (1.2 mL, 8.2 mmol) and methanol (0.5 mL) are added to the crude material obtained above. The solution is heated to 125° C. for 15 minutes in a microwave reaction vessel after which the solution is concentrated in vacuo and the crude product obtained is used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07803827B2 |
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| Source dataset | uspto-grants-2010_09 |
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| ORD ID | ord-05f2b6389e0d4611be9690e55e9a17b5 |
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| Source note | uspto-grants-2010_09 |
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