Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Bromo-2-furanecarboxylic acid → 5-Bromo-furan-2-carboxylic acid (3-cyanomethyl-phenyl)-amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Bromo-2-furanecarboxylic acid | HCID 68511 | — |
| 반응물 | (3-Amino-phenyl)-acetonitrile | HCID 4847850 | — |
| 생성물 | 5-Bromo-furan-2-carboxylic acid (3-cyanomethyl-phenyl)-amide | HCID 59654859 | — |
반응 단계
5-Bromo-furan-2-carboxylic acid (1.68 g, 8.80 mmol) was coupled to aniline (80) (1.16 g, 8.80 mmol), using Method C. The residue was purified by column chromatography eluting with 20% EtOAc in heptane to give the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07803841B2 |
| 출처 데이터셋 | uspto-grants-2010_09 |
| ORD ID | ord-5f97ba9a441e4983ac4c2b582abab1c8 |
| 출처 메모 | uspto-grants-2010_09 |