HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azido(trimethyl)stannane → HCID 178522031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azido(trimethyl)stannane | HCID 5104973 | — |
| Reactant | 5-Bromo-furan-2-carboxylic acid (3-cyanomethyl-phenyl)-amide | HCID 59654859 | — |
| Product | HCID 178522031 | HCID 178522031 | — |
Reaction Steps
Nitrile (83) (162 mg, 0.53 mmol) was treated with Me3SnN3 using Method K. The residue was purified by column chromatography, flushing with heptane (200 ml) and eluting with 50% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803841B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-d984b7d3efdd4c2c938e3809bf181386 |
| Source note | uspto-grants-2010_09 |