HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl 2-(3-aminophenoxy)acetate → (3-{[6-(3-Chloro-phenyl)-pyridine-2-carbonyl]-amino}-phenoxy)-acetic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl 2-(3-aminophenoxy)acetate | HCID 412308 | — |
| Edukt | 6-(3-Chlorophenyl)picolinic acid | HCID 24730135 | — |
| Produkt | (3-{[6-(3-Chloro-phenyl)-pyridine-2-carbonyl]-amino}-phenoxy)-acetic acid ethyl ester | HCID 59654828 | — |
Reaktionsschritte
Carboxylic acid (136) (44 mg, 0.19 mmol) was coupled with aniline (64) (40 mg, 0.2 mmol) using Method D. The residue was purified by column chromatography eluting with 10% EtOAc in heptane to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07803841B2 |
| Quelldatensatz | uspto-grants-2010_09 |
| ORD ID | ord-af0cbb0bdca84406a5653eb1f3fe915f |
| Quellennotiz | uspto-grants-2010_09 |