HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-fluorobenzoic acid → HCID 68499179, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-fluorobenzoic acid | HCID 2736315 | — |
| Reactant | 3-(3-Amino-phenyl)-acrylonitrile | HCID 53425496 | — |
| Product | HCID 68499179 | HCID 68499179 | — |
Reaction Steps
5-Bromo-2-fluoro-benzoic acid (380 mg, 1.74 mmol) was coupled to aniline (88) (250 mg, 1.74 mmol) using Method C. The residue was purified by column chromatography eluting with 20% EtOAc in heptane to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803841B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-5a6fbcccaea943e89947a38b758a0dce |
| Source note | uspto-grants-2010_09 |