HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178502860, compound → HCID 178502859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178502860 | HCID 178502860 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178502859 | HCID 178502859 | — |
Reaction Steps
To a solution of 4-azidomethyl-N-methoxy-benzamidine (11.3 g, 0.055 mol; see step (i) above) in 200 mL of ethanol was added 200 mg of PtO2. The mixture was hydrogenated with constant bubbling of hydrogen for 4 h and subsequently filtered through Celite® and evaporated. Yield: 7.34 g (74%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07803954B2 |
| Source dataset | uspto-grants-2010_09 |
| ORD ID | ord-951c478f96b24d359ce7b3262f9700a1 |
| Source note | uspto-grants-2010_09 |