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1-(3-Chloro-2,4-dihydroxy-phenyl)ethanone → 1-{3-Chloro-2-hydroxy-4-[3-(4-iodo-benzyl)-[1,2,4]oxadiazol-5-ylmethoxy]-phenyl}-ethanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-(3-Chloro-2,4-dihydroxy-phenyl)ethanone | HCID 57438294 | — |
| 反応物 | 5-Chloromethyl-3-(4-iodo-benzyl)-[1,2,4]oxadiazole | HCID 57438413 | — |
| 反応物 | 1-{2-Hydroxy-4-[3-(3-iodo-benzyl)-[1,2,4]oxadiazol-5-ylmethoxy]-3-methyl-phenyl}-ethanone | HCID 66699621 | — |
| 生成物 | 1-{3-Chloro-2-hydroxy-4-[3-(4-iodo-benzyl)-[1,2,4]oxadiazol-5-ylmethoxy]-phenyl}-ethanone | HCID 66699645 | — |
反応手順
The title compound is prepared essentially as described for 1-{2-hydroxy-4-[3-(3-iodo-benzyl)-[1,2,4]oxadiazol-5-ylmethoxy]-3-methyl-phenyl}-ethanone, employing 1-(3-chloro-2,4-dihydroxy-phenyl)-ethanone and 5-Chlormethyl-3-(4-iodo-benzyl)-[1,2,4]oxadiazole. LC-MS (m/e): 485 (M+1).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07803938B2 |
| 出典データセット | uspto-grants-2010_09 |
| ORD ID | ord-ffd87ca85a6f4d548e483f254fa52ce9 |
| 出典メモ | uspto-grants-2010_09 |