HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl(methylene)ammounium iodide → 2-[2-(5-Dimethylaminomethyl-2-thienylmethylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl(methylene)ammounium iodide | HCID 2724133 | — |
| Reactant | 2-[2-(2-Thienylmethylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone | HCID 13505296 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-[2-(5-Dimethylaminomethyl-2-thienylmethylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone | HCID 13505300 | — |
Reaction Steps
2-[2-(2-Thienylmethylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone is reacted with an excess of dimethyl(methylene)ammonium iodide in dimethylformamide at room temperature to give 2-[2-(5-dimethylaminomethyl-2-thienylmethylthio)ethylamino]-5-(3-pyridylmethyl)-4-pyrimidone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539207 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-91f2bbb333514944ae5a81fe860ee538 |
| Source note | uspto-grants-1985_09 |