HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → Ethyl 2-formyl-3-(6-methyl-3-pyridyl)propionate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Ethyl 3-(6-methyl-3-pyridyl)propionate | HCID 3018102 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | Ethyl 2-formyl-3-(6-methyl-3-pyridyl)propionate | HCID 3018359 | — |
Reaction Steps
Ethyl 3-(6-methyl-3-pyridyl)propionate was formylated with ethyl formate and sodium hydride in 1,2-dimethoxyethane to give ethyl 2-formyl-3-(6-methyl-3-pyridyl)propionate m.p. 142°-144°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539207 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-436749c24cfa40f5b093d725965d0824 |
| Source note | uspto-grants-1985_09 |