HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 70457139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 86740278 | HCID 86740278 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 70457139 | HCID 70457139 | — |
Reaction Steps
4-Hydroxy-5,6,7,8-tetrahydro-4-naphthonitrile (1.73 g, 10 mm), isopropyl bromide (0.78 g, 10 mM), and sodium hydride (0.24 g, 10 mM) in dimethyl formamide were stirred for 3 hours. Water was added and the mixture was extracted with ether. The ether was dried and evaporated to give the isopropyl ether (7).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539319 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-89198089e4a34dbf8b5f8f100b64db38 |
| Source note | uspto-grants-1985_09 |