HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilic acid, N-m-nitrophenyl- → 2-(3-Nitroanilino)benzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilic acid, N-m-nitrophenyl- | HCID 101403 | — |
| Reactant | 2-[3-(Trifluoromethyl)anilino]benzoyl chloride | HCID 13231214 | — |
| Product | 2-(3-Nitroanilino)benzoyl chloride | HCID 13231215 | 77% |
Reaction Steps
The following compound is obtained using the same procedure as that used for procurement of 2-(3-trifluoromethylphenylamino)-benzoyl chloride except that an equivalent amount of 2-(3-nitrophenylamino)-benzoic acid is used in place of the 2-(3-trifluoromethylphenylamino)-benzoic acid of the reference example from 2-(3-nitrophenylamino)-benzoic acid: 2-(3-Nitrophenylamino)-benzoyl chloride ##STR9## Yield: 77% of theory, melting point: 141°-145° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539402 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-35a54c85b56d49338f1b0c24175023a0 |
| Source note | uspto-grants-1985_09 |