HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20268268, compound → HCID 13371470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20268268 | HCID 20268268 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13371470 | HCID 13371470 | 55.9% |
Reaction Steps
1-[2-(4-Benzyloxyphenylamino)phenyl]ethanone (9 g) in 900 ml of ethanol and 90 ml of acetic acid was hydrogenated in the presence of 1 g of 10% palladium-on-carbon catalyst. The product was isolated and recrystallized from acetonitrile to yield 3.6 g of 1-[2-(4-hydroxyphenylamino)phenyl]ethanone, orange solid, m.p. 168°-169° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539429 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-06a1f2405f9941e39bc920fc75120192 |
| Source note | uspto-grants-1985_09 |