HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 54399221, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Phenol, 2,2-bis(1,1-dimethylethyl)-6-mercapto- | HCID 3041162 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 54399221 | HCID 54399221 | 57.5% |
Reaction Steps
In a 50 ml flask under nitrogen, a mixture of 5.00 grams of 2,4-di-tert-butyl-6-mercaptophenol, 1.80 grams of methyl acrylate and 20 mls toluene was treated with 0.50 mls of triethylamine. After stirring for three hours at ambient temperature, the solvent was removed in vacuo. The residue was purified by chromatography on silica gel using toluene/heptane eluent to give 3.90 g (57% yield) of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04540732 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-eb1447d37e394e3080212b5acbb4ef17 |
| Source note | uspto-grants-1985_09 |