Ethanol → HCID 20267360, compound

HRID 1719611Notes

Reaction equation

HRID 1719611 reaction equation
Cl.[Cl:2][CH:3]([C:6]1[CH:11]=[CH:10][N:9]=[CH:8][CH:7]=1)[CH2:4]Cl.[CH2:12]([OH:14])[CH3:13]>>[ClH:2].[Cl:2][CH:3]([C:6]1[CH:11]=[CH:10][N:9]=[CH:8][CH:7]=1)[CH2:4][O:14][CH2:12][CH3:13]

Participants

3

Reactant 2

HCID 702EthanolHCID 20267356HCID 20267356, compound

Product 1

HCID 20267360HCID 20267360, compound

Procedure

About 2 g of 4-(1,2-dichloroethyl)pyridine hydrochloride were refluxed in absolute ethanol overnight. Excess ethanol was then evaporated, and the remaining traces were removed on a vacuum pump. The process resulted in the production of 2.5 g of 4-(1-chloro-2-ethoxyethyl)pyridine hydrochloride.

Workup

  1. customExcess ethanol was then evaporated
  2. customthe remaining traces were removed on a vacuum pump

Sources & evidence

ORD record
ord-69cd270fddb04a53b342f85a2d77c55f
Source dataset
uspto-grants-1985_09
Patent number
US04540793

Reaction notes

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