HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20233096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl 2-(phenylamino)acetate | HCID 571509 | — |
| Reactant | HCID 23035632 | HCID 23035632 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 20233096 | HCID 20233096 | — |
Reaction Steps
125 g of N-phenylglycine methyl ester were dissolved in 600 ml of absolute toluene and 161 g of acetylmandelyl chloride, dissolved in 80 ml of toluene, were added dropwise (cooling with ice); a further 76.5 g of triethylamine in 200 ml of toluene were then added dropwise. After 1 hour, water was added and the organic phase was separated off, dried and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04542148 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-03a813a13f6a40a9a81bb877d70f1e9d |
| Source note | uspto-grants-1985_09 |