Ethanol → HCID 178526498, compound

HRID 1719858Notes

Reaction equation

HRID 1719858 reaction equation
[N+:1]([C:4]1[CH:12]=[CH:11][C:7]2[NH:8][N:9]=[N:10][C:6]=2[CH:5]=1)([O-:3])=[O:2].C(O)C.[N+]([O-])([O-])=O.[Ag+:20]>O>[Ag:20].[N+:1]([C:4]1[CH:12]=[CH:11][C:7]2[NH:8][N:9]=[N:10][C:6]=2[CH:5]=1)([O-:3])=[O:2]

Participants

5

Reactant 3

HCID 702EthanolHCID 24470Silver NitrateHCID 178526497HCID 178526497, compound

Product 1

HCID 178526498HCID 178526498, compoundYield 97.1%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Solution was prepared by dissolving 18.0 g (0.11 mole) of 5-nitrobenzotriazole into 300 ml of ethanol and whereto a solution prepared by dissolving 16.9 g (0.10 mole) of silver nitrate into 100 ml of water was dropped and the mixture thereof was stirred for 30 minutes. The crystals thus produced were filtrated and were then washed with 100 ml of ethanol, and thus, 26.4 g of 5-nitrobenzotriazole silver were obtained.

Workup

  1. customSolution was prepared
  2. customwhereto a solution prepared
  3. additionwas dropped
  4. customThe crystals thus produced
  5. filtrationwere filtrated
  6. washwere then washed with 100 ml of ethanol

Sources & evidence

ORD record
ord-702b07eddf9340ea91b60726fb5fb1e5
Source dataset
uspto-grants-1985_09
Patent number
US04543309

Reaction notes

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