HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 19421445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 2,3-Dichloro-6-nitroquinoxaline | HCID 689090 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19421445 | HCID 19421445 | 95% |
Reaction Steps
A mixture of 6.1 g (25 mmol) of 2,3-dichloro-6-nitroquinoxaline and 2.75 g (55 mmol) of hydrazine hydrate in 150 ml of ethanol was stirred at room temperature over night. The precipitate was isolated and washed with water, cold ethanol and ether to give 5.67 g (95%) of crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504085 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-06f2a3e1c0af4406b988aa74c25d1909 |
| Source note | uspto-grants-1996_04 |