HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 22419801, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 22419799 | HCID 22419799 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22419801 | HCID 22419801 | 94% |
Reaction Steps
A mixture of 3.4 g (14.2 mmol) of 3-chloro-2-methoxy-6-nitroquinoxaline and 1.65 g (33 mmol) of hydrazine hydrate in 150 ml of ethanol was stirred at room temperature over night. The precipitate was collected and washed with water and cold ethanol to give 3.13 g (94%) of crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504085 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-bfd46d28e08e487abb7d9d46b0f32e40 |
| Source note | uspto-grants-1996_04 |