HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trimethylbenzaldehyde → HCID 86749382, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trimethylbenzaldehyde | HCID 10254 | — |
| Reactant | Diphenylphosphine oxide | HCID 254003 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86749382 | HCID 86749382 | 98% |
Reaction Steps
To 101 g (0.5 mol) of diphenyl phosphine oxide and 74 g (0.5 mol) of 2,4,6-trimethylbenzaldehyde in 150 mL of toluene there were added 0.5 g of a 30 wt % strength sodium methylate solution. The product began to crystallize after 10 minutes and was isolated in the usual manner. Yield: 98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504236 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-ead92158ec6344d88ac098e2c3832fc6 |
| Source note | uspto-grants-1996_04 |