1,4-Butanediol → ethyl N-{2-(4-hydroxybutoxycarbonyl)benzoyl)carbamate

HRID 1720119Notes

Reaction equation

HRID 1720119 reaction equation
[CH2:1]([O:3][C:4]([N:6]1[C:10](=[O:11])[C:9]2=[CH:12][CH:13]=[CH:14][CH:15]=[C:8]2[C:7]1=[O:16])=[O:5])[CH3:2].[CH2:17]([OH:22])[CH2:18][CH2:19][CH2:20][OH:21]>>[OH:21][CH2:20][CH2:19][CH2:18][CH2:17][O:22][C:7]([C:8]1[CH:15]=[CH:14][CH:13]=[CH:12][C:9]=1[C:10]([NH:6][C:4](=[O:5])[O:3][CH2:1][CH3:2])=[O:11])=[O:16]

Participants

3

Reactant 2

HCID 80641,4-ButanediolHCID 31187N-Carbethoxyphthalimide

Product 1

HCID 22420367ethyl N-{2-(4-hydroxybutoxycarbonyl)benzoyl)carbamate

Procedure

According to the same manner as described in Example 1 except for reacting N-ethoxycarbonylphthalimide with 1,4-butanediol under conditions shown in Table 19, ethyl N-{2-(4-hydroxybutoxycarbonyl)benzoyl)carbamate was obtained. Characteristics and identified structure of the resulting compound are shown in Table 6.

Sources & evidence

ORD record
ord-6197b783d9fd4b8a857ec8ff411b9bac
Source dataset
uspto-grants-1996_04
Patent number
US05504242

Reaction notes

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