HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dioxane, 2-(2-bromoethyl)- → N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| Reactant | 4-(4-Methylstyryl)quinoline | HCID 54172084 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-[2-(1,3-dioxane-2-yl)ethyl]-4-(4-methylstyryl)-quinolinium bromide | HCID 70262692 | 70% |
Reaction Steps
4-(4-methylstyryl) quinoline (0.245 g) and 2-(2-bromoethyl) 1,3-dioxane (0.195 g) were mixed and refluxed in ethylacetate (1.5 ml) for 18 hours. Yellow-green precipitate was separated by filtration, washed with ethyl ether and dried in vacuo to give 0.308 g of N-[2-(1,3-dioxane-2-yl) ethyl]-4-(4-methylstyryl)-quinolinium bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506089 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-a0d0dfdda27248d287e139f8c23622fa |
| Source note | uspto-grants-1996_04 |