HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Phenylethenyl)pyridine → N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Phenylethenyl)pyridine | HCID 101576 | — |
| Reactant | 1,3-Dioxane, 2-(2-bromoethyl)- | HCID 520656 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | N-[2-(1,3-dioxane-2-yl)ethyl]-4-styrylpyridinium bromide | HCID 70260576 | 90.5% |
Reaction Steps
4-styrylpyridine (1.81 g) and 2-(2-bromoethyl) 1,3-dioxane (1.95 g) were stirred and refluxed in ethylacetate (15 ml) solution for 15 hours. After cooling of the reaction mixture creamy crystals were separated by filtration, washed with ethyl ether and dried to give 3.4 g of N-[2- (1,3-dioxane-2-yl) ethyl]-4-styrylpyridinium bromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506089 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-db5c85387f07472b87449c5417851600 |
| Source note | uspto-grants-1996_04 |