HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 53861216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 54555908 | HCID 54555908 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 53861216 | HCID 53861216 | — |
Reaction Steps
An excess of diazomethane in diethylether is added to 3.35 g of 2-vinylnicotinic acid ethyl ester and stirred at -10° overnight. Acetic acid is added until gas evolution ceases and the solvent is removed by evaporation under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506191 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-b2b4f5b7e0e84e54b2d977932361f3a2 |
| Source note | uspto-grants-1996_04 |