HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aniline → 2-oxo-N-phenylpropanehydrazonoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | 3-Chloro-2,4-pentanedione | HCID 74328 | — |
| Reactant | Sodium Nitrite | HCID 23668193 | — |
| Product | 2-oxo-N-phenylpropanehydrazonoyl chloride | HCID 2771522 | 40.3% |
Reaction Steps
The reaction of 10.55 g (0.113 mol)of aminobenzene with 13.2 g of sodium nitrite and 20 g of 3-chloro-2,4-pentanedione as in Example 1 yielded 8.95 g of 1-chloro-1-[(phenyl)hydrazono]-2-propanone, mp 132°-134° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-0de9b627fbae4f3f99c769040638639e |
| Source note | uspto-grants-1996_04 |