HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → 1-[(4-Chlorophenyl)thio]-1-[(phenyl)hydrazono]-2-propanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-oxo-N-phenylpropanehydrazonoyl chloride | HCID 2771522 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-[(4-Chlorophenyl)thio]-1-[(phenyl)hydrazono]-2-propanone | HCID 54223511 | 23.5% |
Reaction Steps
The reaction of 951 mg (4.85 mmol) of 1-chloro-1-[(phenyl) hydrazono]-2-propanone with 864 mg of 4-chlorothiophenol and 840 ul of triethylamine in 15 ml of ethanol as Example 11 yielded 347 mg of 1-[(4-chlorophenyl)thio]-1-[(phenyl)hydrazono]-2-propanone, mp 111°-113° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-8153a6f0c58842128be8f6c71b6fd2e8 |
| Source note | uspto-grants-1996_04 |