HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 22417646, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 22417653 | HCID 22417653 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 22417646 | HCID 22417646 | 86% |
Reaction Steps
The bromide from Step 5 (740 mg, 3.7 mmol) and triphenylphosphine (1.31 g, 5 mmol) were dissolved in acetonitrile (15 mL) and the mixture was refluxed for 6 hours. Evaporation of the solvent in vacuo left a solid that was swished in Et2O. Filtration and vacuum drying of the powder gave 1.46 g (86%) of the desired phosphonium salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506227 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-e474b8d9690a492694844d558c8757ab |
| Source note | uspto-grants-1996_04 |